Zeolite-Based Silica Synthesis With Calcination Temperature Variations 100oC, 150oC and 200oC
DOI:
https://doi.org/10.21580/jnsmr.2018.4.2.11019Keywords:
Zeolit, Silica and XRD (X-Ray Diffraction)Abstract
This research on Zeolite-Based Silica Synthesis with Calcination Temperature Variations 100 , 150 , and 200 . The purpose of this study was to determine the effect of calcination temperature on the silica structure contained in zeolites. Synthesis is made from zeolite, NaOH and HCl by sol-gel method and temperature calcination treatment 100 , 150 , and 200 . Zeolite samples were characterized by XRD (X- Ray Diffraction). The results showed that sample A with temperature 100 contains Quartz silica, moganite silica (SiO2), and Aluminum Oxide (Al2O3). Sample B with temperature 150 contains Quartz silica (SiO2), and Anorthite (AlCaO8Si). Sample C with 200 contains Quartz silica and Aluminium Oxide (Al2O3). As for the crystallite size in sample A measuring 678.51 nm, sample B measuring 488.16 nm and sample C measuring 488.13 nm. ©2018 JNSMR UIN Walisongo. All rights reserved.
Downloads
References
Ardiansyah, Arie. 2015. Synthesis of Nanosilica Using Sol Gel Method and Hydrophobicity Test on Acrylic Paints. Skripsi. Semarang: Jurusan Kimia FMIPA UNNES
Buhani and Suharso.2016. Modification of Silica as Absorbent of Heavy Metal. Yogyakarta: Innosain.
Hadi, Surahmat dan Munasir. 2011. Synthesis of Silica Based on Natural Bancar Sand Using the Coprecipitation Method. Jurusan Fisika FMIPA ITS No: 2.Vol 7.
Kusuma, Hamdan Hadi. 2015. X-Ray Diffraction and Density Distribution Measurements on the Al2O3 Crystals Grown by Czochralski Method with Different Pull Rate. Jurnal of Natural Sciences and Mathematics Research.
Priyanto, Agus.2015. Synthesis and Application of Silica from Petung Bamboo Leaf Ash (Dendrocalamus Asper (Schult.f.) Backer ex Heyne) To Reduce Ammonium and Nitrate Levels in Tofu Liquid Waste. Skripsi. Semarang:FITK UIN Walisongo.
Rahma, Hayati and Astuti. 2015. Synthesis of Silica Nanoparticles from Purus Beach Sand, Padang, West Sumatra Using the Copresitipation Method. Jurusan Fisika Unand No: 03.Vol 4
Rokayah,Siti.2016. Analysis of Structure and Specific Surface Area of Zeolites Based on Rice Husk Silica Due to Calcination Temperature Variations 150℃, 250℃ and 350℃. Skripsi. Lampung: Jurusan Fisika FMIPA Universitas Lampung
Yuliana, Tika and Astuti. 2016. The Effect of Calcination Temperature on the Synthesis of Silica Nanoparticles in Purus Beach, Padang City. Jurnal Fisika Unand No : 04, Vol 05.
Downloads
Published
Issue
Section
License
Copyright
The copyright of the received article shall be assigned to the publisher of the journal. The intended copyright includes the right to publish the article in various forms (including reprints). The journal maintains the publishing rights to published articles. Authors are allowed to use their articles for any legal purposes deemed necessary without written permission from the journal, but with an acknowledgment to this journal of initial publication.
Licensing
